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Optimization of Spray-Drying conditions of microencapsulated habanero pepper (Capsicum chinense Jacq.) extracts and physicochemical characterization of the microcapsules
Kevin Alejandro Avilés Betanzos
JUAN VALERIO CAUICH RODRIGUEZ
MANUEL OCTAVIO RAMIREZ SUCRE
Ingrid Mayanin Rodríguez Buenfil
Acceso Abierto
Atribución-NoComercial-SinDerivadas
https://doi.org/10.3390/pr11041238
OPTIMIZATION
SPRAY DRYING
CAPSICUM CHINENSE
ANTIOXIDANT CAPACITY
POLYPHENOLS
The Habanero pepper (Capsicum chinense Jacq.) is recognized worldwide for its unique organoleptic characteristics, as well as for its capsaicin content; however, other bioactive compounds, such as phenolic compounds with bioactive properties (mainly antioxidant capacity), have been extracted (ultrasound) and identified in this fruit. Moreover, the extracts obtained by ultrasound present a high sensitivity to environmental conditions, making spray drying a viable option to avoid the degradation of bioactive compounds while maintaining their properties after microencapsulation. Response surface methodology (RSM) has been used to optimize spray-drying conditions such as the inlet temperature (IT) and maltodextrin:extract (M:E) ratio. Thus, the objective of this work was to establish the optimal spray-drying conditions (IT and M:E) of a Habanero pepper extract with a final characterization of the spray-dried product. Results showed that the optimal spray-drying conditions included an IT = 148 °C with an M:E = 0.8:1 w/w, where the antioxidant capacity (38.84 ± 0.22% inhibition), total polyphenol content (6.64 ± 0.08 mg Gallic acid equivalent/100 g powder), and several individual polyphenols, such as Protocatechuic acid (26.97 mg/100 g powder), Coumaric acid (2.68 mg/100 g powder), Rutin (18.01 mg/100 g powder), Diosmetin (1.74 mg/100 g powder), and Naringenin (0.98 mg/100 g powder), were evaluated. The microcapsules showed a spherical shape with concavities and moisture less than 5%, and the inclusion of bioactive compounds was confirmed using UPLC and FTIR. The final dried product has the potential to be used as an ingredient for functional food development.
2023
Artículo
Processes. 11, 1238, 2023.
Inglés
Avilés-Betanzos, K.A.; Cauich-Rodríguez, J.V.; Ramírez-Sucre, M.O.; Rodríguez-Buenfil, I.M. Optimization of Spray-Drying Conditions of Microencapsulated Habanero Pepper (Capsicum chinense Jacq.) Extracts and Physicochemical Characterization of the Microcapsules. Processes 2023, 11, 1238. https://doi.org/10.3390/pr11041238
BIOLOGÍA MOLECULAR
Versión publicada
publishedVersion - Versión publicada
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